Novel liquid chromatography method based on linear weighted regression for the fast determination of isoprostane isomers in plasma samples using sensitive tandem mass spectrometry detection | Canada Hyperbarics Skip to main content
Study J Chromatogr B Analyt Technol Biomed Life Sci 2017

Novel liquid chromatography method based on linear weighted regression for the fast determination of isoprostane isomers in plasma samples using sensitive tandem mass spectrometry detection

Aszyk J, Kot J, Tkachenko Y, Woźniak M, Bogucka-Kocka A, Kot-Wasik A — J Chromatogr B Analyt Technol Biomed Life Sci, 2017

Tier 2, Indexed

Automatically imported from PubMed based on relevance criteria.

Summary

What Researchers Did

Researchers developed a new, precise laboratory method to quickly measure four specific markers of oxidative stress called isoprostanes in human blood plasma.

What They Found

The new method achieved very low detection limits, ranging from 1.0 to 2.1 pg/mL for the isoprostanes. It also showed high consistency, with intra-day repeatability between 2.1% and 3.5% and inter-day repeatability between 0.1% and 5.1%. The method was successfully used to monitor isoprostane levels in plasma from 8 young patients exposed to hyperbaric hyperoxia (100% oxygen at 280kPa(a) for 30 minutes).

Canadian Relevance

This study is not Canadian. However, it involves monitoring patients exposed to hyperbaric hyperoxia, which is a key component of hyperbaric oxygen therapy (HBOT) used for several Health Canada-recognised indications.

Study Limitations

The applicability of the method was only tested on a very small group of 8 young patients, limiting the generalizability of the biological findings.

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Study Details

Study Type Study
Category Uncategorised
Source Pubmed
PubMed ID 28282637
Year Published 2017
Journal J Chromatogr B Analyt Technol Biomed Life Sci
MeSH Terms Adult; Biomarkers; Chromatography, High Pressure Liquid; Humans; Hyperoxia; Isomerism; Isoprostanes; Limit of Detection; Linear Models; Liquid-Liquid Extraction; Oxidative Stress; Prostaglandins; Tandem Mass Spectrometry; Young Adult

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Disclaimer: This study summary is provided for informational and educational purposes only. It does not constitute medical advice. The information presented reflects the findings of the original research authors and may not represent the views of Canada Hyperbarics. Always consult a qualified healthcare professional before making treatment decisions.

Last reviewed: April 17, 2026 | Reviewed by: Canada Hyperbarics Editorial Team | Editorial process | Research sources | Counts & methodology